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Lab Notes - Failure in Making Sodium Nitrite

Final version. As usual, i'll post on Saturday, but you all get to see it now :)

Lab Notes - Failure in Making Sodium Nitrite

Comments

its something to a consider. the issue is that such solvents aren't easy to come by for the amateur. but it's definitely something to try.

NurdRage

For the direct hydrolysis, would an aprotic solvent help? Maybe a slow addition to DMSO with a carbonate, or maybe even CaO. Alternately, it might be possible to combine the acid directly with powdered CaO or MgO and a bit of heat to melt it.

Twizzy

yep, of course now the question becomes what sort of interesting diazo compounds can i make? hehehe, i'll see

NurdRage

Can’t isopropyl nitrite be used to make sodium azide? Which in its way is also a useful reagent to get diazo compounds

Mono Keras


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