Lab Notes - Failure in Making Sodium Nitrite
Added 2023-10-19 18:45:51 +0000 UTCFinal version. As usual, i'll post on Saturday, but you all get to see it now :)
Comments
its something to a consider. the issue is that such solvents aren't easy to come by for the amateur. but it's definitely something to try.
NurdRage
2023-10-23 15:33:58 +0000 UTCFor the direct hydrolysis, would an aprotic solvent help? Maybe a slow addition to DMSO with a carbonate, or maybe even CaO. Alternately, it might be possible to combine the acid directly with powdered CaO or MgO and a bit of heat to melt it.
Twizzy
2023-10-23 08:22:50 +0000 UTCyep, of course now the question becomes what sort of interesting diazo compounds can i make? hehehe, i'll see
NurdRage
2023-10-19 20:03:28 +0000 UTCCan’t isopropyl nitrite be used to make sodium azide? Which in its way is also a useful reagent to get diazo compounds
Mono Keras
2023-10-19 19:33:29 +0000 UTC
